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Specifications, Properties, Uses, SDS of Calcium Undecylenate USP Grade Manufacturer Supplier Exporter Wholesale & Small Packs, CAS Number 1322-14-1. |
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Muby Chem Pvt. Ltd. is a several decades old group of companies, engaged in manufacturing, supplying, distributing, wholesale supplies of Calcium Undecylenate for actual users, including retail or small pack supplies for research and development work.
We supply fine and speciality chemicals, pharmaceutical excipients, mineral fortifiers in chemically pure, analytical reagent grade, IP BP USP Ph Eur EP JP and other pharmaceutical grade monograph including FCC Food grade chemicals and Nutraceuticals at best prices. We and/or our associated units have all the facilities to supply as per cGMP standard observing good manufacturing practice and good laboratory practice. We can assure low microbial count and also offer a test certificate for the same. We maintain warehouses across USA, India, and UAE. Our group exports to USA, Canada, Mexico, Argentina, Brazil, Chile, Korea, Malaysia, Thailand, Indonesia, Europe, and several other parts of the world. We supply in wholesale container loads to small pack of few grams. Solid products may be specified for it size and shape as desired by the buyer.
Calcium Undecylenate CAS Number 1322-14-1
For Properties Specifications Uses of Calcium Undecylenate Click Properties, Specifications, Uses, Price, Process of Calcium Undecylenate Manufacturer.
For For SDS MSDS Sheet of Calcium Undecylenate Click SDS Safety Data Sheet MSDS Sheet of Calcium Undecylenate Manufacturer.
The Properties, Specifications, Monograph and Uses of Calcium Undecylenate:
CAS Number: 1322-14-1, EINECS EC Number: 215-331-8, Molecular Formula: C22H38CaO4, Molecular Weight: 406.61 HS Code 29161990
Calcium Undecylenate is also known as Calcium diundec-10-enoate; 10-Undecenoic acid, calcium salt; 10-Undecenoic acid, calcium salt (2:1). It is a very economical anti-fungal agent and is used as an active ingredient in many topical over the counter anti-fungal preparations, both powders and ointments.
Calcium Undecylenate USP Grade Specifications:
C22H38O4Ca --- 406.61
10-Undecenoic acid, calcium (2+) salt;
Calcium 10-undecenoate --- CAS 1322-14-1
DEFINITION
Calcium Undecylenate contains NLT 98.0% and NMT 102.0% of calcium undecylenate (C22H38O4Ca), calculated on the dried basis.
IDENTIFICATION
A. Identification Tests-General, Calcium
Sample solution: A filtered solution (1 in 20) of Calcium Undecylenate in 3 N hydrochloric acid
Acceptance criteria: Meets the requirements
B. Melting Range or Temperature, Class:
Sample solution: Suspend 10 g of Calcium Undecylenate in 40 mL of water in a 250-mL separator. Cautiously and slowly add 10 mL of hydrochloric acid while swirling. Insert the stopper, and shake. The separator will become quite warm, and pressure must be carefully and frequently relieved through the stopcock. If a curdy, white material remains after 5 min of shaking, add additional hydrochloric acid, 1 mL at a time, and shake until a clear oily phase is formed.
Analysis: Allow the phases to separate, drain, and discard the bottom aqueous layer. Drain and discard the middle oily layer if present. Filter the top layer of undecylenic acid through a pledget of cotton, noting the volume obtained. To the filtrate add an equal volume of aniline. Reflux for 1 h, swirling the flask occasionally. Allow to cool and pour 60 mL of alcohol through the condenser into the flask. Remove the flask from the condenser, add 1 g of charcoal, and stir. Filter the slurry. Add water dropwise until a few crystals form or the solution becomes slightly cloudy. If too much water is added, an oil will form. Add alcohol dropwise until the oil dissolves. Allow the mixture to stand or refrigerate until crystals are formed. Collect the crystals on a filter paper inserted in a 45-mm porous glass filter funnel. Wash the crystals with 75 mL of 25% alcohol: the crystals have a clean, white, glossy appearance. If not, recrystallize by dissolving the crystals in about 50 mL of alcohol. Add about 1 g of charcoal, stir, filter, and continue as directed above, beginning with “Add water dropwise”. Dry the crystals under vacuum at 50C for 2 h. If the melting point is low, additional drying or recrystallization may be necessary.
Acceptance criteria: The crystals so obtained melt at 66C –67.5C.
ASSAY
Procedure
Sample solution: Boil 40.0 mL of 0.1 N hydrochloric acid VS with 600 mg of Calcium Undecylenate for 10 min, or until the undecylenic acid layer is clear, adding water as necessary, to maintain the original volume. Transfer the mixture, with the aid of water, to a 500-mL separator. Dilute with water to about 75 mL, and extract with two 100-mL portions of solvent hexane. Wash the combined extracts with water until the last washing is neutral to litmus and add the washings to the original water layer. Cool.
Titrimetric system
Mode: Residual titration
Titrant: 0.1 N hydrochloric acid
Back-titrant: 0.1 N sodium hydroxide VS
Endpoint detection: Visual
Analysis: Add 3 drops of methyl orange to the Sample solution. Then titrate the excess Titrant with Back-titrant. Perform a blank determination. Each mL of hydrochloric acid is equivalent to 20.33 mg of calcium undecylenate (C22H38O4Ca).
Acceptance criteria: 98.0% to 102.0% on the dried basis.
Limit of Free Undecylenic Acid: to pass the test.
Acceptance criteria: NMT 0.1%
Loss on Drying:
Analysis: Dry at 105C for 2 h.
Acceptance criteria: 2.0% to 5.7%
Particle Size Distribution Estimation by Analytical Sieving:
Analysis: Test in accordance with this procedure, except use NMT 25 g and use a single No. 100 sieve that is to be shaken for NLT 30 min or until sifting is practically complete.
Acceptance criteria: NLT 99.0% of it passes through a No. 100 sieve.
Packaging and Storage: Preserve in well-closed containers.
The MSDS-SDS Hazard Statement of Calcium Undecylenate:
Calcium Undecylenate SDS, Safety Data Sheet
MSDS, Material Safety Data Sheet 19-Aug-21
Section 1: Chemical Product and Identification
Product Name & Other Names: Calcium Undecylenate or 10-Undecenoic acid, calcium (2+) salt
CAS#: 1322-14-1
EINECS EC-No.: 215-331-8
Molecular Weight: 406.61
Chemical Formula: C22H38CaO4
Relevant uses and uses advised against (if any): Laboratory and Industrial Manufacturing.
SUPPLIER: As per letterhead.
Section 2: Hazards Identification
GHS, Globally Harmonized System Classification in accordance with 29 CFR 1910
Classification according to Regulation (EC) No 1272/2008
Not a hazardous substance or mixture according to Regulation (EC) No. 1272/2008.
This substance is not classified as dangerous according to Directive 67/548/EEC.
Labeling according to GHS & Regulation (EC) No 1272/2008
GHS Label Elements NONE |
Signal Word: None
Precautionary statements:
P261: Avoid breathing dust/fume/gas/mist/vapors/spray.
P302+P352 - IF ON SKIN: Wash with plenty of soap and water.
P303+P361+P353 - IF ON SKIN (or hair): Remove/Take off immediately all contaminated clothing. Rinse skin with water/shower.
P304 + P340 - IF INHALED: Remove victim to fresh air and keep at rest in a position comfortable for breathing.
P305 + P351 + P338 - IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing.
P337+313: If eye irritation persists get medical advice/attention.
Section 3: Composition and Information on Ingredients
Product Name & Other Names: Calcium Undecylenate or 10-Undecenoic acid, calcium (2+) salt
CAS#: 1322-14-1
EINECS EC-No.: 215-331-8
Section 4: First Aid Measures
Always seek medical attention after first aid measures are provided.
Eye Contact: In case of contact, immediately flush eyes with plenty of water for at least 15 minutes. Get medical attention.
Skin Contact: In case of contact, immediately flush skin with plenty of water. Cover the irritated skin with an emollient. Thoroughly clean shoes and clothes before reuse. Get medical attention.
Inhalation: If Calcium Undecylenate is inhaled, remove to fresh air. If not breathing, give artificial respiration. If breathing is difficult, give oxygen. Get medical attention.
Ingestion: Do NOT induce vomiting unless directed to do so by medical personnel. Never give anything by mouth to an unconscious person. If large quantities of this material are swallowed, call a physician immediately.
Section 5: Fire and Explosion Data
Flammability of the Product: Not a fire hazard. I can be combustible at high temperature.
Auto-Ignition Temperature: Not available.
Products of Combustion: Some metallic oxides CO CO2 and fumes.
Fire Hazards in Presence of Various Substances: Slightly flammable in presence of heat.
Fire Fighting Media and Instructions:
Small Fire: Use DRY chemical powder.
Large Fire: Use water spray, fog, or foam. Avoid water jet.
Extinguishing Media Not recommended: Avoid using solid water jet as it may scatter the fire.
Special Information: In the event of a fire, wear full protective clothing and NIOSH-approved self-contained breathing apparatus with full face piece operated in the pressure demand or other positive pressure mode. At high temperatures under fire conditions, it may produce toxic or irritating fumes. Fire-extinguishing work is done from the windward and the suitable fire-extinguishing method according to the surrounding situation is used. Uninvolved persons should evacuate to a safe place.
Section 6: Accidental Release Measures
Personal precautions, protective equipment, and emergency procedures: Ventilate area of leak or spill. Avoid breathing dust/fumes/gas/mist/vapors/spray. Use individual protective equipment (waterproof boots, suitable protective clothing, safety glasses, etc.). Restrict unprotected personnel from the area. Prevent any contact with hot surfaces. Do not approach facing the wind. Do not touch the spilled material.
Environmental precautions: Do not let the product enter drains, soil, or water sources.
Methods and materials used for containment cleanup procedures and Storage: Contain spilled material. Cover with an inert, non-combustible absorbent material, (e.g., sand, earth, diatomaceous earth, vermiculite). Vacuum or sweep-up and remove to an approved disposal container. Finish cleaning by spreading water on the contaminated surface and allow to evacuate as per law.
Section 7: Handling and Storage
Precautions for safe handling: Apply according to good manufacturing and industrial hygiene practices. Ensure proper ventilation. In case of insufficient ventilation, wear suitable respiratory equipment. Wash thoroughly after handling. Do not drink, eat, or smoke while handling. Avoid contact with skin, eyes, and clothing. Minimize dust generation. Avoid breathing dust/fumes/gas/mist/vapors/spray. Avoid contact with eyes, skin, and clothing. Keep container tightly closed. Avoid ingestion and inhalation. Use individual protective equipment (waterproof boots, suitable protective clothing, safety glasses, etc.). Prevent any contact with hot surfaces.
Conditions for safe storage, including any incompatibilities: Store in cool, dry, and ventilated area away from heat sources and protected from sunlight in tightly closed original container. Keep air contact to a minimum. Store protected from heat, sparks and ignition sources and incompatible materials. Avoid contact with skin and eyes. Avoid inhalation of dust/mist/vapor. Do not store with incompatible materials like strong oxidizing agents.
Section 8: Exposure Controls/Personal Protection
Exposure Limits: Not established.
Ventilation System: A system of local and/or general exhaust is recommended to keep employee exposures as low as possible. Local exhaust ventilation is generally preferred because it can control the emissions of the contaminant at its source, preventing dispersion of it into the general work area.
Personal Respirators (NIOSH Approved): For conditions of use where exposure to dust or mist is apparent and engineering controls are not feasible, a particulate respirator may be worn. For emergencies or instances where the exposure levels are not known, use a full-face positive-pressure, air-supplied respirator.
Skin Protection: Wear protective gloves and clean body-covering clothing.
Eye Protection: Use chemical safety goggles and/or full-face shield where dusting or splashing of solutions is possible. Maintain eye wash fountain and quick-drench facilities in work area.
Other Control Measures: Maintain good housekeeping in work area. Dust deposits on floors and other surfaces may pick up moisture and cause the surfaces to become slippery and present safety hazards. Handle in accordance with good industrial hygiene and safety practice. Wash hands after handling.
Section 9: Physical and Chemical Properties
Appearance: Solid
Odor: Not available.
Odor threshold: Not available.
pH: Not available.
Relative density: Not available.
Melting point/freezing point: Not available.
Initial boiling point and boiling range: Not available.
Flash point: Not available.
Auto-ignition temperature: Not available.
Decomposition temperature: Not available.
Upper/lower flammability or explosive limits: Not available.
Vapor pressure: Not available.
Vapor density: Not available.
Evaporation rate: Not available.
Flammability (solid, gas): Not available.
Partition coefficient: n-octanol/water: Not available.
Solubility(ies): Not available.
Viscosity: Not available.
Molecular Weight: 406.61
Chemical Formula: C22H38CaO4
Section 10: Stability and Reactivity Data
Stability: It is stable.
Conditions of Instability: Excessive heat, dust generation
Incompatibility with various substances: Oxidizing Agents, heat and sunlight.
Special Remarks on Reactivity: Decomposes on heating.
Hazardous decomposition products formed under fire conditions: Carbon oxides, Calcium oxide.
Polymerization: Will not occur.
Section 11: Toxicological Information
Toxicity to Animals: Not available.
Carcinogenicity: No component of this product present at levels greater than or equal to 0.1% is identified as probable or confirmed human carcinogen by IARC, ACGIH, OSHA and NTP.
Mutagenic Effects: Not available.
Teratogenic Effects: Not available.
Environmental Toxicity: Not available.
Section 12: Ecological Information
Toxicity Data: Not available.
Persistence and Degradability: No information available.
Mobility: No information available.
Bioaccumulation/ Accumulation: No information available.
Results of PBT and vPvB assessment: No data available for assessment.
Section 13: Disposal Considerations
Waste Disposal: Waste must be disposed of in accordance legal regulations.
Section 14: Transport Information
Land Transport DOT USA, TDG Canada & ADR/RID Europe: Not dangerous goods.
Sea Transport IMDG/IMO: Not dangerous goods.
Air Transport ICAOIATA: Not dangerous goods.
Section 15: Other Regulatory Information
USA:
California Proposition 65: Not listed.
Section 16 - Additional Information
DISCLAIMER: The information and recommendations set forth herein are presented in good faith and believed correct as of the date hereof. It is compiled from various sources, and it is not necessarily all inclusive nor fully adequate in every circumstance. In addition, these suggestions should not be confused with nor followed in violation of applicable laws, regulations, rules, or insurance requirements applicable. This SDS MSDS sheet is intended only as a guide to the appropriate precautionary handling of the material by a professionally trained person using this product. Individuals receiving the information must exercise their independent judgment in determining its appropriateness for a particular purpose. This shall not constitute a guarantee for any specific product features and shall not establish a legally valid contractual relationship. In no case shall our company be liable to loss or damages by the product user.
Calcium Undecylenate Manufacturers, Suppliers, Exporters, Wholesalers:
King of Chemicals manufacturers
Plot No. 2900/46&47 + 2900/163to167, GIDC, Ankleshwar, Dist. Bharuch, India
India, USA, UAE
TEL: (Office) 91-22-23774610, 91-22-23723564
e-mail: info@kingofchemicals.com
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