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Specifications, Properties, Uses, SDS of Sodium Lauryl Sulfate or Sodium Lauryl Sulphate or Sodium dodecyl sulfate USP NF BP Ph Eur Grade Manufacturer Supplier Exporter Wholesale & Small Packs, CAS Number 151-21-3.
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Sodium Lauryl Sulfate or Sodium Lauryl Sulphate or Sodium dodecyl sulfate CAS Number 151-21-3For Properties Specifications Uses of Sodium Lauryl Sulfate or Sodium Lauryl Sulphate or Sodium dodecyl sulfate Click Properties, Specifications, Uses, Price, Process of Sodium Lauryl Sulfate or Sodium Lauryl Sulphate or Sodium dodecyl sulfate Manufacturer.
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The Properties, Specifications, Monograph and Uses of Sodium Lauryl Sulfate or Sodium Lauryl Sulphate or Sodium dodecyl sulfate :
CAS Number: 151-21-3, EINECS EC Number: 205-788-1, Molecular Formula: NaC12H25SO4, Molecular Weight: 288.37, HS Code 28331990 or 29209000 or 34021190
Sodium dodecyl sulfate (SDS) or sodium lauryl sulfate (SLS), sometimes written sodium laurilsulfate, is a synthetic organic compound with the formula CH3(CH2)11SO4Na. It is an anionic surfactant used in many cleaning and hygiene products. It is used in many domestic cleaning, personal hygiene and cosmetic, pharmaceutical, and food products, as well as of industrial and commercial cleaning and product formulations. Sodium dodecyl sulfate, appearing as its synonym sodium lauryl sulfate (SLS), is considered a generally recognized as safe (GRAS) ingredient for food use according to the USFDA. It is used as an emulsifying agent and whipping aid. Sodium lauryl sulfate is a widely used in the pharmaceutical field as an ionic solubilizer and emulsifier that is suitable for applications in liquid dispersions, solutions, emulsions and micro emulsions, tablets, foams and semi-solids such as creams, lotions and gels.
Sodium Lauryl Sulfate USP NF Grade Specifications:
Sulfuric acid monododecyl ester sodium salt;
Sodium monododecyl sulfate CAS 151-21-3DEFINITION
Sodium Lauryl Sulfate is a mixture of sodium alkyl sulfates consisting chiefly of sodium lauryl sulfate [CH3(CH2)10CH2OSO3Na]. It contains NLT 85.0% of sodium alkyl sulfates calculated as C12H25NaO4S.IDENTIFICATION
A. Identification Tests-General, Sodium: To pass the test.
B. Identification Tests-General, Sulfate: To pass the test.
C.
Sample: 0.1 g
Analysis: Dissolve the Sample in 10 mL of water and shake.
Acceptance criteria: A copious foam is formed.
D.
Sample: Solution prepared for Identification test C
Analysis: To 0.1 mL of the Sample, add 0.1 mL of a 1 g/L solution of methylene blue and 2 mL of sulfuric acid, diluted. Add 2 mL of methylene chloride and shake.
Acceptance criteria: An intense blue color develops in the methylene chloride layer.ASSAY
Sodium Chloride:
Content of Sodium Alkyl Sulfates:
Methylene blue solution: Dissolve 0.003 g of methylene blue, 5.0 g of anhydrous sodium sulfate, and 1.2 g of sulfuric acid in 100 mL of water.
[Note: Anhydrous sodium sulfate is the emulsion breaker.]
Sample: 1.5 g of Sodium Lauryl Sulfate
Titrimetric system
Mode: Direct titration
Titrant: 0.004 M benzethonium chloride
Endpoint detection: Visual
Analysis
Dissolve the Sample in water, warming if necessary, and dilute with water to exactly 1000.0 mL. To 10.0 mL of the solution, add 25 mL of Methylene blue solution, 15 mL of methylene chloride, and 20 mL of water. Titrate with Titrant, shaking vigorously and allowing the layers to separate before each addition, until the two layers are almost the same blue color. One mL of Titrant is equivalent to 1.154 mg of sodium alkyl sulfates, calculated as C12H25NaO4S.
Acceptance criteria: NLT 85.0%, calculated as C12H25NaO4S
Fluorescein sodium solution: Dissolve 0.2 g of fluorescein sodium in water to 100 mL.
Dilute nitric acid: Dilute 105 mL of nitric acid with water to 1000 mL.
Sample solution: 100 mg/mL of Sodium Lauryl Sulfate in water
Analysis: Neutralize 50 mL of Sample solution with Dilute nitric acid, using litmus paper as the indicator. If necessary, add exactly 5.0 mL of 0.1 N sodium chloride and titrate with 0.1 N silver nitrate VS (indicator: 2 drops of Fluorescein sodium solution) to the first appearance of turbidity with solution color change from yellow green to orange through yellow. Perform a blank determination and make any necessary correction. Each mL of 0.1 N silver nitrate is equivalent to 5.844 mg of sodium chloride.
Acceptance criteria: The combined content of sodium chloride and sodium sulfate is NMT 8.0%.
Sodium Sulfate:
Sample solution: 100 mg/mL of Sodium Lauryl Sulfate in water
Analysis: To 10 mL of Sample solution, add 100 mL of alcohol and heat at a temperature just below the boiling point for 2 h. Pass through a glass filter (pore size equivalent to 5 to 10 µm) while hot, and wash with 100 mL of boiling alcohol. Dissolve the precipitate by washing with 150 mL of water, collecting the washings in a beaker. Add 10 mL of hydrochloric acid, diluted, heat to boiling, add 25 mL of barium chloride and allow to stand overnight. Collect the precipitate and wash with water until the last washing shows no opalescence with 0.1 N silver nitrate. Dry the precipitate, ignite to constant mass between 500C and 600C by raising the temperature gradually, and weigh as barium sulfate (BaSO4; 233.39).
Amount (mg) of sodium sulfate (Na2SO4) = amount (mg) of barium sulfate (BaSO4) x 0.6086
Acceptance criteria: The combined content of sodium chloride and sodium sulfate is NMT 8.0%.
Alkalinity:
Sample solution: Dissolve 1.0 g in 100 mL of water, add 0.1 mL of phenol red TS, and titrate with 0.10 N hydrochloric acid.
Acceptance criteria: NMT 0.5 mL for neutralization
Total Alcohols: Transfer 5 g to an 800-mL Kjeldahl flask, and add 150 mL of water, 50 mL of hydrochloric acid, and a few boiling chips. Attach a reflux condenser to the Kjeldahl flask, heat carefully to avoid excessive frothing, and boil for 4 h. Cool the flask, rinse the condenser with ether, collecting the ether in the flask, and transfer the contents to a 500-mL separator, rinsing the flask twice with ether and adding the washings to the separator. Extract the solution with two 75-mL portions of ether, evaporate the combined ether extracts in a tared beaker on a steam bath, dry the residue at 105C for 30 min, cool, and weigh.
Acceptance criteria: The residue represents the total alcohols and is NLT 59.0% of the weight of Sodium Lauryl Sulfate taken.
Unsulfated Alcohols:
Sample solution: Dissolve 10 g in 100 mL of water and add 100 mL of alcohol.
Analysis: Transfer the solution to a separator, and extract with three 50-mL portions of petroleum ether. If an emulsion forms, sodium chloride may be added to promote separation of the two layers. Wash the combined petroleum ether extracts with three 50-mL portions of water, and dry with anhydrous sodium sulfate. Filter the petroleum ether extract into a tared beaker. Evaporate on a water bath until the odor of petroleum ether no longer is perceptible, dry the residue at 105C for 30 min, cool, and weigh.
Acceptance criteria: The weight of the residue is NMT 4.0% of the weight of Sodium Lauryl Sulfate taken.
Packaging and Storage: Preserve in well-closed containers.
Specifications of Sodium Lauryl Sulphate BP Ph Eur Grade
Ph Eur
Sodium Dodecyl Sulphate
Sodium Laurilsulfate, Ph Eur
Action and use: Anionic emulsifying agent.DEFINITION
Mixture of sodium alkyl sulphates consisting chiefly of sodium dodecyl sulphate (C12H25NaO4S; Mr 288.4).
Content: sodium alkyl sulphates: minimum 85.0 per cent, expressed as C12H25NaO4S.CHARACTERS
Appearance: White or pale yellow, powder or crystals.
Solubility: Freely soluble in water giving an opalescent solution, partly soluble in ethanol (96 per cent).IDENTIFICATION
A. Dissolve 0.1 g in 10 ml of water R and shake. A copious foam is formed.
B. To 0.1 ml of the solution prepared for identification test A, add 0.1 ml of a 1 g/l solution of methylene blue and 2 ml of dilute sulphuric acid. Add 2 ml of methylene chloride and shake. An intense blue colour develops in the methylene chloride layer.
C. Mix about 10 mg with 10 ml of anhydrous ethanol. Heat to boiling on a water-bath, shaking frequently. Filter immediately and evaporate the ethanol. Dissolve the residue in 8 ml of water, add 3 ml of dilute hydrochloric acid, evaporate the solution to half its volume and allow to cool. Separate the congealed fatty alcohols by filtration. To the filtrate add 1 ml of barium chloride solution. A white, crystalline precipitate is formed.
D. Ignite 0.5 g. The residue gives reaction of sodium.TESTS
Alkalinity: Dissolve 1.0 g in 100 ml of carbon dioxide-free water and add 0.1 ml of phenol red solution. Not more than 0.5 ml of 0.1 M hydrochloric acid is required to change the colour of the indicator.
Non-esterified alcohol: Maximum 4 per cent.
Sodium chloride and sodium sulphate: Maximum 8.0 per cent for the total percentage content.
Sodium chloride: Dissolve 5.00 g in 50 ml of water, add dilute nitric acid dropwise until the solution is neutral to blue litmus paper, add 2 ml of potassium chromate solution and titrate with 0.1 M silver nitrate.
1 ml of 0.1 M silver nitrate is equivalent to 5.844 mg of NaCl.
Sodium sulphate: Dissolve 0.500 g in 20 ml of water, warming gently if necessary, then add 1 ml.
The MSDS-SDS Hazard Statement of Sodium Lauryl Sulfate or Sodium Lauryl Sulphate or Sodium dodecyl sulfate :
Sodium lauryl sulfate or Sodium dodecyl sulphate SDS, Safety Data Sheet
MSDS, Material Safety Data Sheet 17-Nov-20SECTION 1. PRODUCT IDENTIFICATION
Product Name & Other Names: Sodium lauryl sulfate or Sodium dodecyl sulfate or Sodium lauryl sulphate or Sodium dodecyl sulphate.
Synonyms: Lauryl sulfate sodium salt, Sodium lauryl sulphate, Dodecyl sodium sulphate, Dodecyl sulfate sodium salt.
CAS Number: 151-21-3
EINECS EC Number: 205-788-1
Molecular Formula: NaC12H25SO4
Molecular Weight: 288.37
Relevant uses and uses advised against (if any): Industrial Manufacturing.
Supplier: As per the letterhead.SECTION 2. HAZARDS IDENTIFICATION
GHS, Globally Harmonized System Classification in accordance with 29 CFR 1910
Classification according to Regulation (EC) No 1272/2008Flammable solids (Category 1), H228
Acute toxicity, oral (Category 4), H302
Acute toxicity, inhalation (Category 4), H332
Skin corrosion/irritation (Category 2), H315
Serious eye damage (Category 1), H318
Specific target organ toxicity, single exposure; Respiratory tract irritation (Category 3), H335
Hazardous to the aquatic environment, acute hazard (Category 2), H401Labeling according to GHS USA & Regulation (EC) No 1272/2008
GHS Label Elements
Flammable SolidsGHS Label Elements
CorrosiveSignal Words: Danger
Hazard statements:
H228: Flammable solid.
H302 + H332: Harmful if swallowed
H315: Causes skin irritation.
H318: Causes serious eye damage.
H335: May cause respiratory irritation.
H401: Toxic to aquatic life.Precautionary statements:
P210: Keep away from heat/sparks/open flames/hot surfaces – No smoking.
P240: Ground/bond container and receiving equipment.
P241: Use explosion-proof electrical/ventilating/light/…/equipment.
P261: Avoid breathing dust/ fume/ gas/ mist/ vapors/ spray.
P262: Do not get in eyes, on skin, or on clothing.
P264 Wash skin thoroughly after handling.
P270: Do not eat, drink or smoke when using this product.
P271: Use only outdoors or in a well-ventilated area.
P273: Avoid release to the environment.
P280: Wear protective gloves/protective clothing/eye protection/face protection.
P330: Rinse mouth.
P301+P312: IF SWALLOWED: Call a POISON CENTER or doctor/physician if you feel unwell.
P302+P352: IF ON SKIN: Wash with soap and water.
P304+340: IF INHALED: Remove victim to fresh air and keep at rest in a position comfortable for breathing.
P305+P351+P338: IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing.
P314: Get Medical advice/attention if you feel unwell.
P337+P313: If eye irritation persists: Get medical advice/ attention.
P370+378: In case of fire: Use water spray, alcohol-resistant foam, dry chemical, or carbon dioxide for extinction.
P391: Collect spillage.
P501: Dispose of contents/ container to an approved waste disposal plant.SECTION 3. COMPOSITION / INFORMATION ON INGREDIENTS
Product Name & Other Names: Sodium lauryl sulfate or Sodium dodecyl sulfate or Sodium lauryl sulphate or Sodium dodecyl sulphate.
Synonyms: Lauryl sulfate sodium salt, Sodium lauryl sulphate, Dodecyl sodium sulphate, Dodecyl sulfate sodium salt.
CAS Number: 151-21-3
EINECS EC Number: 205-788-1SECTION 4. FIRST AID MEASURES
Always seek medical attention after first aid measures are provided.
Eye Contact: Do not allow victim to rub eye (s). Let the eye (s) water naturally for a few minutes. If particle/dust does not dislodge, flush with lukewarm, gently flowing water for 5 minutes or until particle/dust is removed, while holding eyelid (s) open. If irritation persists, obtain medical attention. DO NOT attempt to manually remove anything stuck to the eye.
Skin Contact: Remove contaminated clothing, shoes and leather goods (e.g., watchbands, belts). Quickly and gently blot or brush away excess chemical. Wash gently and thoroughly with lukewarm gently flowing water and non-abrasive soap for 5 minutes. If irritation persists, repeat flushing. Obtain medical advice. Completely decontaminate clothing, shoes and leather goods before reuse or else discard.
Inhalation: If symptoms are experienced, remove source of contamination or move victim to fresh air. Obtain medical advice.
Ingestion: Never give anything by mouth if victim is rapidly losing consciousness or is unconscious or convulsing. Have victim rinse mouth thoroughly with water. DO NOT INDUCE VOMITING. Have victim drink 2 – 8 oz. (60 – 240 ml) of water.SECTION 5. FIRE FIGHTING MEASURES
Fire and Explosion Hazards: Flammable Solids.
Extinguishing Media: Use means of extinction appropriate for the surrounding fire conditions such as water spray, carbon dioxide, dry chemical, or foam.
Extinguishing Media Not recommended: Avoid using solid water jet as it may scatter the fire.
Special Information: In the event of a fire, wear full protective clothing and NIOSH-approved self-contained breathing apparatus with full face piece operated in the pressure demand or other positive pressure mode. At high temperatures under fire conditions, it may produce toxic or irritating fumes. Fire-extinguishing work is done from the windward and the suitable fire-extinguishing method according to the surrounding situation is used. Uninvolved persons should evacuate to a safe place. Do not use water directly on material. Do not allow water run-off to enter sewers or watercourses. Use water spray to cool unopened containers.SECTION 6. ACCIDENTAL RELEASE MEASURES
Procedures for Cleanup: Stop release, if possible, to do so safely. Contain spill, isolate hazard area, and deny entry. Sweep up or vacuum. Place contaminated material in suitable, labeled containers for final disposal. Dispose of waste material consistent with the requirements of waste disposal authorities.
Personal Precautions: Gloves and coveralls or other protective clothing are recommended for persons responding to an accidental release. Close-fitting safety goggles may be necessary in some circumstances to prevent eye contact.
Environmental Precautions: This product can pose a threat to the environment. Contamination of soil and water should be prevented. Keep spillage from entering soil, streams, or sewers.SECTION 7. HANDLING AND STORAGE
Precautions for safe handling: Apply according to good manufacturing and industrial hygiene practices. Ensure proper ventilation. Wash thoroughly after handling. Do not drink, eat, or smoke while handling. Avoid contact with skin, eyes, and clothing. Minimize dust generation. Avoid breathing dust/fumes/gas/mist/vapors/spray. Avoid contact with eyes, skin, and clothing. Keep container tightly closed. Avoid ingestion and inhalation. Use individual protective equipment (waterproof boots, suitable protective clothing, safety glasses, etc.). Prevent any contact with hot surfaces.
Conditions for safe storage, including any incompatibilities: Keep away from sources of ignition - No smoking. Take measures to prevent the build-up of electrostatic charge. Store in cool, dry, and ventilated area away from heat sources and protected from sunlight in tightly closed original container. Keep air contact to a minimum. generating dust and the release of dust into the workplace. Do not leave the material container open. Store protected from heat, sparks and ignition sources and incompatible materials. Avoid contact with skin and eyes. Do not store with incompatible materials like oxidizing agents.SECTION 8. EXPOSURE CONTROLS / PERSONAL PROTECTION
Exposure Limits: This product does not contain any hazardous materials with occupational exposure limits established by the region-specific regulatory bodies.
Ventilation System: A system of local and/or general exhaust is recommended to keep employee exposures as low as possible. Local exhaust ventilation is generally preferred because it can control the emissions of the contaminant at its source, preventing dispersion of it into the general work area.
Personal Respirators (NIOSH Approved): For conditions of use where exposure to dust or mist is apparent and engineering controls are not feasible, a particulate respirator may be worn. For emergencies or instances where the exposure levels are not known, use a full-face positive-pressure, air-supplied respirator.
Skin Protection: Wear protective gloves and clean body-covering clothing.
Eye Protection: Use chemical safety goggles and/or full-face shield where dusting or splashing of solutions is possible. Maintain eye wash fountain and quick-drench facilities in work area.
Other Control Measures: Maintain good housekeeping in work area. Dust deposits on floors and other surfaces may pick up moisture and cause the surfaces to become slippery and present safety hazards. Handle in accordance with good industrial hygiene and safety practice. Wash hands after handling.SECTION 9. PHYSICAL AND CHEMICAL PROPERTIES
Appearance: It is colorless, solid.
Odor: Odorless.
Odor threshold: Not available.
pH: 9 to 10 @ 10% solution.
Relative density: 0.37.
Melting point/freezing point: 204C - 207C.
Initial boiling point and boiling range: Not available.
Flash point: Not available.
Auto-ignition temperature: Not available.
Decomposition temperature: Not available.
Upper/lower flammability or explosive limits: Not available.
Vapor pressure: Negligible @ 20C.
Vapor density: Not available.
Evaporation rate: Not available.
Flammability (solid, gas): Not available.
Partition coefficient: n-octanol/water: Not available.
Solubility(ies): Soluble in water.
Viscosity: Not available.
Molecular Formula: NaC12H25SO4
Molecular Weight: 288.37SECTION 10. STABILITY AND REACTIVITY
Stability and Reactivity: Stable and not considered reactive under normal temperatures and pressures. Hazardous polymerization or runaway reactions will not occur.
Incompatibilities: Oxidizing agents. Avoid excessive heat.
Hazardous Decomposition Products: High temperature operations will generate carbon oxide fume. Under such conditions, sulfur dioxide will also be generated and can cause respiratory distress.SECTION 11. TOXICOLOGICAL INFORMATION
Acute Toxicity (Oral LD50): > 1,200 mg/kg Rat
LC50 Inhalation - Rat - 1 h - > 3,900 mg/m3
Carcinogenicity: No component of this product present at levels greater than or equal to 0.1% is identified as possible or confirmed human carcinogen by IARC, ACGIH, OSHA and NTP.
Teratogenic Effects: Not available.
Mutagenic Effects: Not available.
Developmental Toxicity: Not available.
Reproductive Effects: No information available.
The sodium salt of dodecyl sulfate has been reported to cause pulmonary sensitization resulting in hyperactive airway dysfunction and pulmonary allergy accompanied by fatigue, malaise, and aching.SECTION 12. ECOLOGICAL INFORMATION
Toxicity to fish: flow-through test LC50 - Pimephales promelas (fathead minnow) - 29 mg/l-96 h
Toxicity to daphnia and other aquatic invertebrates: flow-through test EC50 - Daphnia dubia (water flea) - 5.55 mg/l - 48 h
Persistence and Degradability: Readily biodegradable.
Mobility: Likely to be mobile due to water solubility.
Bioaccumulation/ Accumulation: No information available.
Results of PBT and vPvB assessment: No data available for assessment.SECTION 13. DISPOSAL CONSIDERATIONS
Do not wash the material down drain. Put uncontaminated material back into the process if possible. Place contaminated material in suitable, labeled containers for disposal. Dispose of waste material consistent with the requirements of waste disposal authorities.
SECTION 14. TRANSPORT INFORMATION
Land Transport DOT USA, TDG Canada & ADR/RID Europe:
UN Number: 1325
UN proper shipping name: Flammable solids, organic, n.o.s. (Sodium dodecyl sulphate)
Transport hazard class(es): 4.1; Packaging group: III
Air Transport ICAO/IATA:
UN Number: 1325
UN proper shipping name: Flammable solids, organic, n.o.s. (Sodium dodecyl sulphate)
Transport hazard class(es): 4.1; Packaging group: III
Sea Transport IMDG/IMO:
UN Number: 1325
UN proper shipping name: Flammable solids, organic, n.o.s. (Sodium dodecyl sulphate)
Transport hazard class(es): 4.1; Packaging group: IIISECTION 15. REGULATORY INFORMATION
USA Regulations:
SARA 311/312 Hazards: Fire Hazard, Acute Health Hazard. See section 2.
California Prop. 65 Components: This product does not contain any chemicals known to State of California to cause cancer, birth defects, or any other reproductive harm.SECTION 16 - ADDITIONAL INFORMATION
DISCLAIMER: The information and recommendations set forth herein are presented in good faith and believed correct as of the date hereof. It is compiled from various sources, and it is not necessarily all inclusive nor fully adequate in every circumstance. In addition, these suggestions should not be confused with nor followed in violation of applicable laws, regulations, rules, or insurance requirements applicable. This SDS MSDS sheet is intended only as a guide to the appropriate precautionary handling of the material by a professionally trained person using this product. Individuals receiving the information must exercise their independent judgment in determining its appropriateness for a particular purpose. This shall not constitute a guarantee for any specific product features and shall not establish a legally valid contractual relationship. In no case shall our company be liable to loss or damages by the product user.
Sodium Lauryl Sulfate or Sodium Lauryl Sulphate or Sodium dodecyl sulfate Manufacturers, Suppliers, Exporters, Wholesalers:
King of Chemicals manufacturers
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India, USA, UAE
TEL: (Office) 91-22-23774610, 91-22-23723564e-mail: info@kingofchemicals.com
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We and our associates manufacture pure chemicals surpassing Monograph Specifications of Analytical Reagent Standards, British & European Pharmacopoeia BP Ph Eur EP Standard, US Pharmacopoeia USP NF Standard, Indian Pharmacopoeia IP Standard, Japan Pharmacopoeia JP Standard, FCC Food Grade Standard.Dodecyl Gallate or Lauryl Gallate
Hydrated Sodium Glycerophosphate